Nova Terra 52

FLQDGR )RUPDWLRQ ZHUH FROOHFWHG IRU JHRFKHPLFDO DQG LVRWRSLF 6U 1G DQDO\VHV 7HQ PHWDYROFDQLF URFNV DQG IRXU PHWDJUDQLWHV 6DPSOLQJ DLPHG WR FROOHFW WKH PRVW UHSUHVHQWDWLYH DQG XQGLVWXUEHG URFNV DYRLGLQJ VHFWLRQV D൵HFWHG E\ ODWH IUDFWXULQJ DQG ÀXLG SHUFRODWLRQ 7KH UH VXOWV RI WKLV UHVHDUFK KDYH EHHQ GHULYHG LQ D VWLOO XQSXEOL VKHG PDQXVFULSW WKDW FRQVWLWXWHV &KDSWHU RI WKLV 3K' 7KHVLV 6HYHUDO DQDO\WLFDO PHWKRGRORJLHV KDYH EHHQ DSSOLHG WR WKH PDWHULDOV FRQIRUP WR WKH (GLDFDUDQ &DPEULDQ EDVH PHQW RI WKH VWXG\ DUHD $ VLJQL¿FDQW YDULHW\ DQG TXDQWLW\ RI JHRFKHPLFDO LVRWRSLF DQG JHRFKURQRORJLFDO GDWD KDYH EHHQ REWDLQHG ZKLFK VXSSRUW WKH PDLQ UHVXOWV LQFOXGHG LQ WKLV 'RFWRUDO 7KHVLV :KROH URFN JHRFKHPLFDO DQG LVRWR SLF 6P 1G GDWD DUH SUHVHQWHG IRU D WRWDO RI QLQHW\ WKUHH VDPSOHV RI ZKLFK VL[W\ VL[ LQFOXGH 5E 6U LVRWRSLF GDWD 2Q WKH RWKHU KDQG 8 3E JHRFKURQRORJ\ GDWD DUH SURYL GHG RQ ¿YH VDPSOHV ,Q DGGLWLRQ RWKHU WHFKQLTXHV KDYH EHHQ XVHG WR D OHVVHU H[WHQW DQG DSSHDU GHVFULEHG DW WKH HQG RI WKLV FKDSWHU DQG LQ IXUWKHU GHWDLO LQ ODWHU FKDSWHUV 2.2. Main analytical methodologies 6DPSOH SUHSDUDWLRQ :KROH URFN FUXVKLQJ $OO VHOHFWHG VDPSOHV IRU WKLV PHWKRGRORJ\ ZHUH SUHSD UHG LQ WKH 6DPSOH 3UHSDUDWLRQ /DERUDWRULHV RI WKH 0LQHUD ORJ\ DQG 3HWURORJ\ 'HSDUWPHQW DW WKH )DFXOW\ RI *HRORJ\ 8QLYHUVLGDG &RPSOXWHQVH GH 0DGULG 7KH XVXDO VDPSOH SUHSDUDWLRQ SURFHGXUH IRU ZKROH URFN FKHPLFDO DQG LVRWR SLF 1G 6U DQDO\VLV UHTXLUHV UHPRYLQJ DQG RU FOHDQLQJ WKRVH SDUWV WKDW FRQWDLQ ELRORJLFDO UHPDLQV DQG RU VLJQL ¿FDQW ZHDWKHULQJ 2QFH FOHDQHG WKH URFN LV FUXVKHG LQWR SLHFHV RI VPDOO VL]H 7KHVH IUDJPHQWV DUH LQWURGXFHG LQWR WKH VWHHO MDZ JULQGHU DQG FUXVKHG WR REWDLQ VDPSOH SRU WLRQV RI URXJKO\ FHQWLPHWUHV $ 7XQJVWHQ VWHHO GLVF SXOYHUL]HV WKHVH IUDFWLRQV XS WR WKH UHTXLUHG JUDLQ VL]H 7KH SRZGHUHG VDPSOH LV UHSHDWHGO\ TXDUWHUHG WR REWDLQ D UHSUHVHQWDWLYH SRUWLRQ 7KLV IUDFWLRQ LV ¿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p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¿QG WKH SRLQWV RI ODVHU LQFLGHQFH RQ WKH ]LU cons. :KROH URFN JHRFKHPLVWU\ 0DMRU DQG WUDFH HOHPHQWV DQDO\VLV ,Q RUGHU WR REWDLQ WKH ZKROH URFN FKHPLVWU\ PDMRU DQG WUDFH DQDO\VLV WKH SXOYHUL]HG VDPSOHV ZHUH VHQW WR $FWLYDWLRQ /DERUDWRULHV /WG $&7/$%6 KWWS ZZZ &KDSWHU