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Table Ig2-Hf

Lu, Yb and Hf LA-MC-ICPMS data of zircon crystals from sample GCH-26

176

Yb

a

176

Lu

a

178

Hf

180

Hf Sig

Hf

b 176

Hf

176

Hf

d

“ ı

c

T

DM

e

age

f

“ ı U-Pb

g

Lu-Hf

h

177

Hf

177

Hf

177

Hf

177

Hf

(V)

177

Hf

177

Hf

(t)

İ+I (Ga) (Ma) (Ma) conc seq

GCH-26_60

0.0657 57 0

.00230 15 1.46706 1

.88660 6 0.282659 38 0.282639 5.4 1.3 0.84 476 7 91 6

GCH-26_59

0.0324 35 0

.00114 10 1.46711

1.88663 6 0.282301 32 0.282290 -6.2 1.1 1.50 509 8 91 6

GCH-26_58

0.0481 42 0

.00165 11 1.46711

1.88659 5 0.282685 30 0.282669 7.1 1.1 0.77 504 10 95 6

GCH-26_57

0.0149 13 0.00060 4 1.46710 1.88652 8 0.282678 28 0.282674 4.7 1.0 0.81 386 7 95 6

GCH-26_56

0.0099 9 0.00040 3 1.46707 1.88659 8 0.282710 26 0.282707 6.0 0.9 0.74 392 6 93 6

GCH-26_54

0

.0036 3 0.00015 1 1

.46698 1.88641 7 0.282656 34 0.282655 5.2 1.2 0.82 438 8 65 6

GCH-26_53

0.0108 10 0.00056 4 1.46702 1.88634 5 0.282695 38 0.282684 19.8 1.3 0.50 1042 343 52 6

GCH-26_52

0.0622 55 0

.00213 15 1.46704 1

.88645 4 0.282633 38 0.282614 4.5 1.3 0.89 474 7 84 6

GCH-26_51

0

.0057 6 0.00022 2 1

.46712 1.88667 6 0.282655 34 0.282654 3.8 1.2 0.85 379 8 95 6

GCH-26_50

0.0114 10 0.00038 3 1.46714 1.88672 6 0.282705 25 0.282702 6.3 0.9 0.74 415 7 57 6

GCH-26_49

0.0162 28 0.

00062 10 1.46704 1.

88660 6 0.282680 30 0.282673 9.1 1.1 0.72 585 14 95 6

GCH-26_48

0.0669 60 0

.00226 16 1.46692 1

.88610 3 0.282655 41 0.282630 7.6 1.4 0.81 585 9 93

6

GCH-26_47

0

.0055 6 0.00027 3 1

.46713 1.88684 6 0.282647 31 0.282645 3.3 1.1 0.87 372 18 74 6

GCH-26_46

0.0357 30 0

.00129 8 1.46715

1.88666 4 0.282661 37 0.282648 6.3 1.3 0.81 501 7 103 6

GCH-26_45

0

.0093 9 0.00033 3 1

.46708 1.88659 6 0.282687 27 0.282684 6.0 0.9 0.77 432 9 64 6

GCH-26_44

0.0494 42 0

.00171 11 1.46715

1.88656 5 0.282645 37 0.282630 4.5 1.3 0.87 450 7 76 6

GCH-26_43

0

.0070 6 0.00026 2

1.46706 1.88656 7 0.282710 32 0.282708 5.6 1.1 0.74 374 17 64 6

GCH-26_42

0.0218 20 0

.00125 9 1.46722

1.88669 6 0.282658 33 0.282648 4.5 1.2 0.84 417 7 89 6

GCH-26_41

0.0550 101 0

.00193 33 1.46718

1.88661 4 0.282674 45 0.282656 6.5 1.6 0.79 497 7 100 6

GCH-26_40

0.0121 11 0.00067 5 1.46699 1.88652 6 0.282680 33 0.282675 5.5 1.2 0.79 423 31 68 6

GCH-26_39

0.0403 33 0

.00143 9 1.46708

1.88634 4 0.282690 41 0.282677 7.5 1.4 0.75 509 7 90 6

GCH-26_38

0.0250 21 0.00098 6 1.46703 1.88649 4 0.282569 39 0.282530 37.8 1.4 0.31 2062 240 27 6

GCH-26_32

0.0356 56 0

.00122 18 1.46719

1.88666 4 0.282679 35 0.282667 7.3 1.3 0.77 513 7 91 6

GCH-26_31

0.0130 15 0.00059 6 1.46708 1.88673 6 0.282705 31 0.282700 6.3 1.1 0.74 418 9 83 6

GCH-26_30

0.0028 3 0.

00013 1 1.46710 1.

88680 6 0.282667 31 0.282666 4.2 1.1 0.82 379 6 93 6

GCH-26_29

0.0409 46 0

.00143 14 1.46701

1.88673 4 0.282259 36 0.282246 -8.4 1.3 1.60 477 7 70 6

GCH-26_28

0.0137 11 0.00038 2 1.46704 1.88647 7 0.282714 29 0.282711 6.3 1.0 0.73 402 6 100 6

GCH-26_27

0.0217 22 0.00080 7 1.46710 1.88670 4 0.282651 37 0.282644 5.7 1.3 0.83 478 7 96 6

GCH-26_26

0

.0064 7 0.00026 2 1

.46698 1.88644 5 0.282687 33 0.282685 4.6 1.2 0.79 366 96 42 6

GCH-26_25

0

.0056 6 0.00023 2 1

.46706 1.88670 6 0.282696 34 0.282695 5.2 1.2 0.77 379 6 95 6

GCH-26_24

0

.0058 5 0.00024 1 1

.46703 1.88650 7 0.282685 31 0.282683 5.1 1.1 0.79 391 8 100 6

GCH-26_23

0.0596 48 0

.00204 13 1.46697

1.88625 4 0.282649 38 0.282629 6.3 1.4 0.83 531 9 96 6

GCH-26_22

0

.0065 6 0.00022 2 1

.46708 1.88665 6 0.282690 27 0.282688 5.3 1.0 0.77 393 6 93

6

GCH-26_21

0

.0074 7 0.00029 2

1.46713 1.88658 7 0.282685 28 0.282683 4.9 1.0 0.79 379 20 96 6

GCH-26_20

0.0112 10 0.00036 3 1.46707 1.88658 7 0.282696 26 0.282694 5.7 0.9 0.76 400 7 94 6

GCH-26_19

0.0630 78 0

.00194 19 1.46697

1.88634 5 0.282646 34 0.282629 5.1 1.2 0.86 478 7 109 6

GCH-26_18

0.0108 9 0.00039 2 1.46705 1.88671 7 0.282660 23 0.282657 5.0 0.8 0.82 426 12 57 6

GCH-26_17

0.0102 10 0.00038 3 1.46707 1.88669 6 0.282665 22 0.282663 4.4 0.8 0.83 391 9 91 6

GCH-26_16

0.0099 9 0.00036 3 1.46699 1.88643 6 0.282685 30 0.282683 5.0 1.1 0.79 388 6 96

6

GCH-26_15

0.0169 15 0.00064 5 1.46699 1.88632 6 0.282668 42 0.282663 4.3 1.5 0.83 387 7 97 6

GCH-26_14

0

.0034 3 0.00015 1 1

.46711 1.88660 7 0.282698 31 0.282696 11.1 1.1 0.66 639 11 93 6

GCH-26_13

0

.0052 5 0.00025 2 1

.46697 1.88628 6 0.282684 47 0.282683 4.6 1.7 0.80 371 17 1133 6

GCH-26_12

0.0080 8 0.00030 2 1.46711 1.88650 8 0.282685 28 0.282685 -0.7 1.0 0.89 130 8 32 6

GCH-26_11

0.0372 34 0

.00137 10 1.46704

1.88644 5 0.282546 31 0.282532 2.6 1.1 1.03 518 7 99 6

GCH-26_10

0

.0060 5 0.00023 2 1

.46707 1.88660 8 0.282691 24 0.282690 5.4 0.8 0.77 395 6 91 6

GCH-26_9

0.0421 37 0

.00137 9 1.46704

1.88651 4 0.282643 41 0.282629 6.2 1.4 0.84 524 8 104 6

GCH-26_8

0

.0012 1 0.00004 0

1.46707 1.88652 6 0.282662 26 0.282662 5.5 0.9 0.81 444 7 84 6

GCH-26_7

0

.0090 8 0.00032 3 1

.46711 1.88668 8 0.282649 21 0.282646 3.7 0.8 0.86 387 6 95 6

GCH-26_6

0.0206 38 0.

00066 10 1.46718 1.

88664 8 0.282669 24 0.282664 4.7 0.9 0.82 403 9 104 6

İ+I

(t)

d

Grain

“ ı

“ ı

±2ı

c

Quoted uncertainties (absolute) relate to the last quoted figure. The effect of the inter-element fractionation on Lu/Hf was estimated to be about 6 % or less

based on analyses of the GJ-ϭ ĂŶĚ WůĞƐŽǀŝēĞ njŝƌĐŽŶ͘ ĐĐƵƌĂĐLJ ĂŶĚ ƌĞƉƌŽĚƵĐŝďŝůŝƚLJ ǁĂƐ ĐŚĞĐŬĞĚ ďLJ ƌĞƉĞĂƚĞĚ ĂŶĂůLJƐĞƐ ŽĨ ƌĞĨĞƌĞŶĐĞ njircon GJ-ϭ ĂŶĚ WůĞƐŽǀŝēĞ

(data given as mean with 2 standard deviation uncertainties).

(a)

176

Yb/

177

Hf = (

176

Yb/

173

Yb)

true

x (

173

Yb/

177

Hf)

meas

x (M

173(Yb)

/M

177(Hf)

)

ɴ;,ĨͿ

͕ ɴ;,ĨͿ с ůŶ;;

179

Hf/

177

Hf

true

)/(

179

Hf/

177

Hf

measured

)) / ln(M

179(Hf)

/M

177(Hf)

), M = mass of

respective isotopes. The

176

Lu/

177

Hf was calculated in a similar way using

175

Lu/

177

,Ĩ ĂŶĚ ɴ;zďͿ͘

(b)

Mean Hf signal in volts.

(c)

Uncertainties are quadratic additions of the within-run precision and the daily reproducibility of the 40ppb-JMC475 solution. Uncertainties for the JMC475

quoted at 2SD (2 standard deviation).

(d)

Initial

176

Hf/

177

,Ĩ ĂŶĚ ɸ,Ĩ ĐĂůĐƵůĂƚĞĚ ƵƐŝŶŐ ƚŚĞ ĂƉƉĂƌĞŶƚ h-Pb age determined by LA-ICP-MSdating (see column f), and the CHUR parameters:

176

Lu/

177

Hf =

0.0336, and

176

Hf/

177

Hf = 0.282785 (Bouvier et al. 2008).

(e)

Two stage model age in Ga using measured

176

Lu/

177

Lu of each spot (first stage = age of zircon), a value of 0.0113 for the average continental crust (second

stage, values compiled from Rudnick and Gao (2003), and depleted mantle

176

Lu/

177

Lu = 0.0379, and

176

Hf/

177

Hf = 0.283164.

(f)

Apparent U-Pb age determined by LA-ICP-MS.

(g)

U-Pb age concordance (%).

(h)

Sequence in which Lu-Hf analyses were performed. Standard analyses for each sequence are showed on Table 12.

321